3-Chloroperoxybenzoic Acid CAS# 937-14-4
3-Chloroperoxybenzoic Acid CAS# 937-14-4 - Image 2
3-Chloroperoxybenzoic Acid CAS# 937-14-4 - Image 3
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3-Chloroperoxybenzoic Acid CAS# 937-14-4

3-Chloroperoxybenzoic acid (m-CPBA) is a carboxylic acid derivative, a white powder crystal, almost insoluble in water, conveniently soluble in ethanol, ether, soluble in chloroform, dichloroethane. Steady to warm, the annual disintegration price is listed below 1% at room temperature level. Disintegration rate is accelerated in liquid state.

In a polyethylene container, include 1.5 g of magnesium sulfate heptahydrate, 36g of sodium hydroxide, 360ml of water, 90ml of 30% hydrogen peroxide, 450ml of dioxane as well as ice cubes, reduced the temperature level to 15 ° C, as well as include 52.5 g of M-chlorobenzoyl chloride, after that include ice to keep the temperature level listed below 25 ° C. After reacting for 15 mins, include 900ml of 20% chilly sulfuric acid. After standing still, the organic layer was divided, filteringed system, and the filtrate was evaporated to eliminate the solvent (high vacuum cleaner distillation) to get 51g of 3-chloroperbenzoic acid.

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3-Chloroperoxybenzoic Acid CAS# 937-14-4

3-Chloroperoxybenzoic acid Basic information
Chemical Properties Uses
Product Name: 3-Chloroperoxybenzoic acid
Synonyms: 3-CHLOROPEROXYBENZOIC ACID;3-Chloroperoxy benzoic acid(more than 57% but not more than 86%,with 3-chorobenzoic acid);3-Chloroperoxybenzoic acid, balance 3-Chlorobenzoic acid and water, 70-75%;3-Chloroperoxybenzoic acid, 70 – 75%, (balance 3-chlorobenzoic acid and water);3-Chlorobenzeneperoxycarboxylic acid;3-Chloroperoxybenzoic Acid (contains min. 17% Water and min. 6% 3-Chlorobenzoic Acid);3-Chloroperoxybenzoic Acid (contains ca. 30% Water);3-Chloroperoxybenzoic acid ,75%
CAS: 937-14-4
MF: C7H5ClO3
MW: 172.57
EINECS: 213-322-3
Product Categories: Organic Peroxide;Oxidation;Synthetic Organic Chemistry;Organic acids;PHARMACEUTICAL INTERMEDIATES;Aromatics;bc0001;top
Mol File: 937-14-4.mol
3-Chloroperoxybenzoic acid Structure
3-Chloroperoxybenzoic acid Chemical Properties
Melting point 69-71 °C(lit.)
Boiling point 244.67°C (rough estimate)
density 0.56
vapor pressure 0.373Pa at 25℃
refractive index 1.4580 (estimate)
storage temp. 2-8°C
solubility Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
pka 7.57 (in water @ 25 °C)
form Moist Powder
color White
PH 4.5@25 °C (saturated aq. sol)
Odor slight pungent odor
Water Solubility insoluble
Decomposition >88 °C
BRN 608317
Stability: Strong oxidizing agent – contact with combustible material may cause fire. May be shock or heat sensitive. Incompatible with organic materials, strong reducing agents.
InChIKey NHQDETIJWKXCTC-UHFFFAOYSA-N
LogP 1.03 at 25℃
CAS DataBase Reference 937-14-4(CAS DataBase Reference)
NIST Chemistry Reference 3-Chloroperbenzoic acid(937-14-4)
EPA Substance Registry System Benzenecarboperoxoic acid, 3-chloro- (937-14-4)

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